Ethyl 2-oxocyclohexylacetate → HCID 23043100, compound
Reaction equation
Cl.[Cl:2][C:3]1[CH:19]=[CH:18][C:6]([CH2:7][N:8]([C:10]2[CH:15]=[CH:14][C:13]([Cl:16])=[CH:12][C:11]=2[Cl:17])N)=[CH:5][CH:4]=1.[CH3:20][CH2:21][O:22][C:23]([CH2:25][CH:26]1[C:31](=O)[CH2:30][CH2:29][CH2:28][CH2:27]1)=[O:24]>>[Cl:2][C:3]1[CH:19]=[CH:18][C:6]([CH2:7][N:8]2[C:27]3[CH:26]([CH2:25][C:23]([O:22][CH2:21][CH3:20])=[O:24])[CH2:31][CH2:30][CH2:29][C:28]=3[C:15]3[C:10]2=[C:11]([Cl:17])[CH:12]=[C:13]([Cl:16])[CH:14]=3)=[CH:5][CH:4]=1Participants
3
Procedure
Following the procedure of Example 1, but using 1-(4-chlorobenzyl)-1-(2,4-dichlorophenyl)hydrazine hydrochloride and ethyl 2-cyclohexanone acetate as starting materials, the title compound is prepared.
Sources & evidence
- ORD record
- ord-3886f6fd8c0e4da0ab867e9c9a4b9c0a
- Source dataset
- uspto-grants-1990_07
- Patent number
- US04940719
Reaction notes
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