Ethyl 2-oxocyclohexylacetate → HCID 23043103, compound

HRID 2165582Notes

Reaction equation

HRID 2165582 reaction equation
Cl.[Cl:2][C:3]1[CH:21]=[CH:20][C:6]([CH2:7][N:8]([C:10]2[CH:15]=[CH:14][C:13]([C:16]([F:19])([F:18])[F:17])=[CH:12][CH:11]=2)N)=[CH:5][CH:4]=1.[CH3:22][CH2:23][O:24][C:25]([CH2:27][CH:28]1[C:33](=O)[CH2:32][CH2:31][CH2:30][CH2:29]1)=[O:26]>>[Cl:2][C:3]1[CH:21]=[CH:20][C:6]([CH2:7][N:8]2[C:29]3[CH:28]([CH2:27][C:25]([O:24][CH2:23][CH3:22])=[O:26])[CH2:33][CH2:32][CH2:31][C:30]=3[C:15]3[C:10]2=[CH:11][CH:12]=[C:13]([C:16]([F:19])([F:18])[F:17])[CH:14]=3)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 91229Ethyl 2-oxocyclohexylacetateHCID 21273600HCID 21273600, compound

Product 1

HCID 23043103HCID 23043103, compound

Procedure

Following the procedure of Example 1, but using 1-(4-chlorobenzyl)-1-(4-trifluoromethylphenyl) hydrazine hydrochloride and ethyl 2-cyclohexanone acetate as starting materials, the title compound was prepared as a mixture of ethyl and isopropyl esters.

Sources & evidence

ORD record
ord-a9690c7d597e497f87b1ba2ff87ef2d8
Source dataset
uspto-grants-1990_07
Patent number
US04940719

Reaction notes

Loading…