Ethyl 2-oxocyclohexylacetate → HCID 131716465, compound

HRID 2165589Notes

Reaction equation

HRID 2165589 reaction equation
[ClH:1].[CH3:2][C:3]1[CH:8]=[C:7]([CH3:9])[CH:6]=[CH:5][C:4]=1[NH:10]N.C[CH2:13][O:14][C:15]([CH2:17][CH:18]1[C:23](=O)[CH2:22][CH2:21][CH2:20][CH2:19]1)=[O:16]>>[Cl:1][C:6]1[CH:7]=[CH:8][C:3]([CH2:2][N:10]2[C:23]3[CH:18]([CH2:17][C:15]([O:14][CH3:13])=[O:16])[CH2:19][CH2:20][CH2:21][C:22]=3[C:5]3[C:4]2=[C:3]([CH3:2])[CH:8]=[C:7]([CH3:9])[CH:6]=3)=[CH:4][CH:5]=1

Participants

3

Procedure

Following the procedure of Example 30, but using 1-(2,4-dimethylphenyl) hydrazine hydrochloride and ethyl 2-cyclohexanone acetate in Step I, as starting materisl, the title compound is prepared.

Sources & evidence

ORD record
ord-4569f00469744084b47e7228add1306f
Source dataset
uspto-grants-1990_07
Patent number
US04940719

Reaction notes

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