反应详情

N'-t-butyl-N-(2-furoyl)hydrazine (1.0 g) was dissolved in 10 ml toluene and 2 ml water. 50% aqueous sodium hydroxide (1.0 g) was added followed by benzoylchloride (0.8 g). After stirring for 14 hours at room temperature, the solid product, N'-t-butyl-N-(2-furoyl)-N'-benzoylhydrazine, was removed by filtration and washed with water: m.p. 160°-162° C.

1. customthe solid product, N'-t-butyl-N-(2-furoyl)-N'-benzoylhydrazine, was removed by filtration
2. washwashed with water