Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 3-Bromo-4-chloroquinoline | HCID 618306 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14209234 | HCID 14209234 | — |
Reaction Steps
A mixture of 9.1 g of 3-bromo-4-chloro-quinoline and 2.0 g of ethanolamine was heated at 150° C. for 30 minutes. The reaction mixture was cooled, 60 ml of water was added and the precipitate was collected by filtration and recrystallized from isopropanol. The yield was 9.5 g, mp 163°-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04942168 |
|---|
| Source dataset | uspto-grants-1990_07 |
|---|
| ORD ID | ord-6fca810ac1d84b04894d4a3b496f08df |
|---|
| Source note | uspto-grants-1990_07 |
|---|
