HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethoxyethylamine → N-(2-Ethoxyethyl)-3-nitropyridin-2-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethoxyethylamine | HCID 66970 | — |
| Edukt | 2-Chloro-3-nitropyridine | HCID 79613 | — |
| Edukt | Sodium Bicarbonate | HCID 516892 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | N-(2-Ethoxyethyl)-3-nitropyridin-2-amine | HCID 15718757 | 100% |
Reaktionsschritte
A mixture of 19 parts of 2-chloro-3-nitropyridine, 13.5 parts of 2-ethoxyethanamine, 13 parts of sodium hydrogen carbonate and 240 parts of ethanol was stirred for 6 hours at reflux temperature. After cooling, the mixture was filtered over diatomaceous earth and the filtrate was evaporated, yielding 25.5 parts (100%) of N-(2-ethoxyethyl)-3-nitro-2-pyridinamine as a residue (interm. 8).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04943580 |
| Quelldatensatz | uspto-grants-1990_07 |
| ORD ID | ord-0609d0acf0f1408b97b6bf6148c314cc |
| Quellennotiz | uspto-grants-1990_07 |