Benzylamine → N-[5-(2-Phenylethoxy)pentyl]benzenemethanamine

HRID 2166159Notes

Reaction equation

Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][O:7][CH2:8][CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[CH2:16]([NH2:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:10]1([CH2:9][CH2:8][O:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][NH:23][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

Reactant 2

HCID 7504Benzylamine

HCID 197980262-(5-Bromopentoxy)ethylbenzene

Product 1

HCID 20062790N-[5-(2-Phenylethoxy)pentyl]benzenemethanamine

Procedure

N-[5-(2-Phenylethoxy)pentyl]benzenemethanamine (8.6 g) was prepared in a similar manner from [2-[(5-bromopentyl)oxy]ethyl]benzene (10 g) and benzylamine (30 ml). The undistilled product was used without further purification in Example 1(c).

Workup

distillationThe undistilled product was used without further purification in Example 1(c)

Sources & evidence

ORD record: ord-6f7a477d80444cfebad50c1f20fadd40
Source dataset: uspto-grants-1990_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04943591

Reaction notes

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