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HRID2166170

反应详情

EQUATION

反应方程式

HRID 2166170 的结构方程式

REACTANTS

反应物

2
结构：O=C(c1ccc(I)cc1)N1CCOCC1
HCID772634

未命名化合物

结构：C#CCOCCCCCCNCc1ccccc1
HCID19101838

N-Benzyl-6-[(prop-2-yn-1-yl)oxy]hexan-1-amine

C16H23NO

PRODUCTS

生成物

1
结构：O=C(c1ccc(C#CCOCCCCCCNCc2ccccc2)cc1)N1CCOCC1
HCID23042177

未命名化合物

收率 40.4%

PROCEDURE

实验过程

4-(4-Iodobenzoyl)morpholine (4.0 g) and N-[6-[(2-propynyl)oxy]- hexyl]benzenemethanamine (3.09 g) were reacted according to the method of Intermediate 31. FCC purification eluting with ethyl acetate-triethylamine (100:1) gave the title compound as a yellow oil (2.21 g), t.l.c. (Ethyl acetate-triethylamine 100:1) Rf 0.2.

WORKUP

后处理

  1. customFCC purification
  2. washeluting with ethyl acetate-triethylamine (100:1)