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HRID2166255

反应详情

EQUATION

反应方程式

HRID 2166255 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)CC(C)(C)c1ccc(O)c(N=Nc2ccccc2[N+](=O)[O-])c1
HCID103927

2-((2-Nitrophenyl)azo)-4-(1,1,3,3-tetramethylbutyl)phenol

C20H25N3O3

结构：CCC(C)(C)c1cc(N=Nc2ccccc2[N+](=O)[O-])c(O)c(C(C)(C)CC)c1
HCID104111

2,4-Bis(2-methylbutan-2-yl)-6-[(2-nitrophenyl)diazenyl]phenol

C22H29N3O3

PRODUCTS

生成物

1
结构：CC(C)(C)CC(C)(C)c1ccc(O)c(-n2nc3ccccc3[n+]2[O-])c1
HCID14297368

未命名化合物

收率 90%

PROCEDURE

实验过程

The same procedure as in Example 1 was repeated, except that 2-nitro-2'-hydroxy-3',5'-di-t-amylazobenzene 25.5 g was replaced by 2-nitro-2'-hydroxy-5'-t-octylazobenzene 23.7 g, thus producing 20.3 g of 2-(2-hydroxy-5-t-octylphenyl)benzotriazole-N-oxide having a melting point of 106° to 110° C. at the yield of 90.0%.