Tributylstannane → HCID 88609037, compound

Participants

Reaction Steps

Following the procedure of Example 63, reduction of 1-deoxy-1-(diethoxyphosphinyl)-1,1-difluoro-3,4,6-tris-O-(phenylmethyl)-D-fructofuranosyl chloride with tributyltin hydride, followed by column chromatography of the crude product gave the desired compound, the more polar component, as an oil, CMR δ 77.9 (doublet of triplets, O-C-CF2P).

Provenance & Evidence