HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 15747283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 14820086 | HCID 14820086 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15747283 | HCID 15747283 | — |
Reaction Steps
A mixture of 3.06 g of 6-(4-acetyl-5-hydroxy-2-allylphenoxy)hexanoic acid, 1.74 ml of oxalyl chloride, 100 ml of methylene chloride, and ten drops of dimethylformamide was mixed at 0° C. and allowed to warm to room temperature. After stirring for 4 hours, the solvents were removed by evaporation to provide the desired title product. NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04945099 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-386748a83228428fbdbac97dbe28658f |
| Source note | uspto-grants-1990_07 |