HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14820055, compound → HCID 14820120, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14820055 | HCID 14820055 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 14820120 | HCID 14820120 | 98.5% |
Reaction Steps
A mixture of 2.0 g of 5-(4-acetyl-2-ethyl-5-hydroxyphenoxy)pentanenitrile, 50 ml of acetic acid, and 2.0 g of 10% palladium on carbon were subjected to on for approximately 2 hours. The mixture was then filtered and concentrated in vacuo. The residue was triturated with diethyl ether to provide 2 g of the desired title product, m.p.=75°-76° C. NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04945099 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-d4b82d1f2d374231b12a966e7f72f7a3 |
| Source note | uspto-grants-1990_07 |