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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2166399Generated: October 30, 2026

HCID 14820055, compound → HCID 14820120, compound

https://huagongshe.com/reaction/2166399

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 14820055HCID 14820055—
CatalystPalladiumHCID 23938—
SolventAcetic AcidHCID 176—
ProductHCID 14820120HCID 1482012098.5%

Reaction Steps

A mixture of 2.0 g of 5-(4-acetyl-2-ethyl-5-hydroxyphenoxy)pentanenitrile, 50 ml of acetic acid, and 2.0 g of 10% palladium on carbon were subjected to on for approximately 2 hours. The mixture was then filtered and concentrated in vacuo. The residue was triturated with diethyl ether to provide 2 g of the desired title product, m.p.=75°-76° C. NMR.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04945099
Source datasetuspto-grants-1990_07
ORD IDord-d4b82d1f2d374231b12a966e7f72f7a3
Source noteuspto-grants-1990_07