8-Bromooctanoic acid → HCID 23039662, compound

HRID 2166434Notes

Reaction equation

HRID 2166434 reaction equation
[C:1]([O:18][CH2:19][C:20](=[CH2:23])[CH2:21][OH:22])(=[O:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[Br:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][C:32](O)=[O:33]>>[C:1]([O:18][CH2:19][C:20](=[CH2:23])[CH2:21][O:22][C:32](=[O:33])[CH2:31][CH2:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][Br:24])(=[O:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 5482758-Bromooctanoic acidHCID 23039641HCID 23039641, compound

Product 1

HCID 23039662HCID 23039662, compound

Procedure

Following the procedure described in Preparation 9, but replacing 3-octadecylaminocarbonyloxy-2-methylenepropan-1-ol with 3-hexadecanoyloxy-2-methylenepropan-1-ol (from Preparation 2), and replacing 6-bromohexanoic acid with 8-bromooctanoic acid, the desired product was obtained.

Workup

  1. customdescribed in Preparation 9

Sources & evidence

ORD record
ord-0d29ba0a279c4696b675c76808f752be
Source dataset
uspto-grants-1990_07
Patent number
US04945098

Reaction notes

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