6-Bromohexanoic acid → HCID 23039618, compound

HRID 2166436Notes

Reaction equation

HRID 2166436 reaction equation
[CH2:1]([O:19][C:20]([O:22][CH2:23][C:24](=[CH2:27])[CH2:25][OH:26])=[O:21])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].BrCCCCCC(O)=O.[Br:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][C:44](O)=[O:45]>>[CH2:1]([O:19][C:20]([O:22][CH2:23][C:24](=[CH2:27])[CH2:25][O:26][C:44](=[O:45])[CH2:43][CH2:42][CH2:41][CH2:40][CH2:39][CH2:38][Br:37])=[O:21])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

4

Reactant 3

HCID 202106-Bromohexanoic acidHCID 1217237-Bromoheptanoic acidHCID 23039644HCID 23039644, compound

Product 1

HCID 23039618HCID 23039618, compound

Procedure

Following the procedure described in Preparation 9, but replacing 3-octadecylaminocarbonyloxy-2-methylenepropan-1-ol with 3-octadecyloxycarbonyloxy-2-methylenepropan-1-ol and 6-bromohexanoic acid with 7-bromoheptanoic acid, the desired product was obtained.

Workup

  1. customdescribed in Preparation 9

Sources & evidence

ORD record
ord-324b7e199bea4aa3b5a618b84a885ba3
Source dataset
uspto-grants-1990_07
Patent number
US04945098

Reaction notes

Loading…