HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzylamine → 1,1-Dibenzyl-3-(2,4-dimethylphenyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzylamine | HCID 7656 | — |
| Reactant | 1-isocyanato-2,4-dimethylbenzene | HCID 5207585 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 1,1-Dibenzyl-3-(2,4-dimethylphenyl)urea | HCID 17381625 | — |
Reaction Steps
A solution of 4.89 g. of 2,4-dimethylphenylisocyanate in 100 ml. of hexane is added to a solution of 5.32 g. of dibenzylamine in 150 ml. of hexane and the solution is stirred at room temperature for 2 hours and then evaporated. The residual solid is recrystallized from pentane to yield 1,1-dibenzyl-3-(2,4-dimethylphenyl)urea, m.p. 124°-126° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04387106 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-dd2a7e784d464e0680873980dbc70537 |
| Source note | uspto-grants-1983_06 |