Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Naphthalene | HCID 931 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-Phenylmaleimide | HCID 13662 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | 2-Allylphenol | HCID 15624 | — |
| Product | HCID 86738922 | HCID 86738922 | — |
Reaction Steps
A 2-allylphenol-N-phenylmaleimide copolymer was prepared by conventional free radical solution polymerization. A solution of 51.60 g N-phenylmaleimide and 1.48 g azobisisobutyronitrile in 100 g THF was added over two hours to a heated (79° C.) solution of 0.76 g naphthalene in 40.00 g 2-allylphenol under nitrogen. The solution was heated an additional 24 hours at 74° C., then cooled, and added to diethyl ether. The polymer was filtered and dried. Conversion was to 73%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04388451 |
|---|
| Source dataset | uspto-grants-1983_06 |
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| ORD ID | ord-5bb58d865fc7457daa1599f1778ff614 |
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| Source note | uspto-grants-1983_06 |
|---|
