Dichloromethane → HCID 86738925, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 3.00 ml of allylamine, 30 ml of CH2Cl2, 5.85 ml of triethylamine and 5.81 ml of BOC-azide is prepared at 0° C. and stirred at 25° C. for 16.5 hours while protected from moisture. It is then treated with 2 ml of water for 20 minutes, evaporated, treated with ethyl acetate, extracted successively with water, aqueous pH 2 phosphate buffer, water, aqueous K2HPO4 and brine, dried with MgSO4, filtered and evaporated to afford 5.54 g of product, m.p. 37° C.

Provenance & Evidence