HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzonitrile → HCID 178420165, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzonitrile | HCID 7505 | — |
| Reactant | Hydrazine | HCID 9321 | — |
| Product | HCID 178420165 | HCID 178420165 | 20.3% |
Reaction Steps
Benzonitrile (52 ml, 0.5 mole) and anhydrous hydrazine (16 ml, 0.5 mole) were heated at 90°-109° C. for 14 hours under nitrogen gas to give an orange solid. Recrystallization from toluene gave 12 g of orange-pink solid of melting point 177°-178° C. (compared to literature mp of 181° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04389327 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-0120b925144c4d5782371ab7aecbd9bb |
| Source note | uspto-grants-1983_06 |