HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Tetrachloride → 5-Chloromethylfurfural
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 5-(Hydroxymethyl)furfural | HCID 237332 | — |
| Product | 5-Chloromethylfurfural | HCID 74191 | — |
Reaction Steps
A mixture of 5-hydroxymethylfurfuraldehyde (0.5 g, 4 mmol) and triphenylphosphine (1.3 g, 5 mmol) in dry carbon tetrachloride (3 ml) was heated at reflux for 30 min and then filtered to give an unstable 1 M solution of 5-chloromethylfurfuraldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04389410 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-122b197f3a2b44d0ab3a21146c897447 |
| Source note | uspto-grants-1983_06 |