HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[2-Chloro-4-(2-diethylaminoethoxy)phenyl]-2-methylene-1-butanone → 1-[2-Chloro-4-(3-diethylaminopropoxy)phenyl]-2-methylene-1-butanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[2-Chloro-4-(2-diethylaminoethoxy)phenyl]-2-methylene-1-butanone | HCID 13052372 | — |
| Reactant | 1-[2-Chloro-4-(3-diethylaminopropoxy)phenyl]-1-butanone | HCID 20497165 | — |
| Product | 1-[2-Chloro-4-(3-diethylaminopropoxy)phenyl]-2-methylene-1-butanone | HCID 13052376 | — |
Reaction Steps
This compound is prepared by essentially the same method as described in Example 1 Step B except that the 1-[2-chloro-4-(2-diethylaminoethoxy)phenyl]-1-butanone of Example 1 Step B is replaced by an equimolecular quantity of 1-[2-chloro-4-(3-diethylaminopropoxy)phenyl]-1-butanone. The product is obtained as a yellow oil upon distillation in vacuo (0.4 mm.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04390537 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-9f4b995023bd4ffa9847f8121f9567cb |
| Source note | uspto-grants-1983_06 |