HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → Alpha-Ionone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 2-(4-Keto-2,6,6-trimethylcyclohex-2-en-1-yl)ethanol | HCID 20489863 | — |
| Reactant | 1,5,5-Trimethyl-9-oxa-bicyclo[4.3.0]non-2-ene | HCID 20489866 | — |
| Reactant | Hexahydro-4,4,7a-trimethyl-6(2H)-benzofuranone | HCID 20489867 | — |
| Product | Alpha-Ionone | HCID 5282108 | — |
Reaction Steps
Identification has been carried out by mass spectrum as stated above. The composition can be characterized by the presence of compounds 1 [2-(4-hydroxy-2,6,6-trimethylcyclohex-2-en-1-yl)ethanol] and 2 [2-(4-keto-2,6,6-trimethylcyclohex-2-en-1-yl)ethanol] and especially 3 [1,5,5-trimethyl-9-oxa-bicyclo[4.3.0]non-2-ene] and 4 [1,5,5-trimethyl-9-oxa-bicyclo[4.3.0]nonan-3-one]. (See Table A).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04390556 |
| Source dataset | uspto-grants-1983_06 |
| ORD ID | ord-f9835eb404fc4739ae65b5ac7c073a09 |
| Source note | uspto-grants-1983_06 |