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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2167190Generated: November 1, 2026

HCID 86627645, compound → HCID 86627646, compound

https://huagongshe.com/reaction/2167190

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86627645HCID 86627645—
SolventMethanolHCID 887—
ProductHCID 86627646HCID 8662764699.9%

Reaction Steps

Crude 4-{5-chloro-2-[(2-chloro-pyridine-4-carbonyl)-amino]phenyl}-3,6-dihydro-2H-pyridine-1-carboxylic acid 1-chloro-ethyl ester (550 mg) was dissolved in methanol (25 ml) in and heated to reflux for 16 hours. Evaporation afforded the crude title product (465 mg). Retention Time HPLC 1.48 min; MS (ES+) 350, 348 (M+H+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09045422B2
Source datasetuspto-grants-2015_06
ORD IDord-c8e04b132df743a0942f2d288f65b82b
Source noteuspto-grants-2015_06