HCID 89885064, compound → HCID 89795742, compound

Participants

Reaction Steps

Similar to the preparation of 27a, the reaction of 25 with 26e afforded the desired compound 27e (8.0 mg, 7%) as oil. TLC Rf: 0.35 (20% EtOAc/petroleum ether); 1H NMR (400 MHz, CDCl3): δ 5.14-5.09 (m, 3H), 4.25-4.20 (m, 1H), 3.95-3.90 (m, 3H), 2.20-1.60 (m, 28H), 0.99-0.97 (m, 3H), 0.89-0.87 (m, 3H). LCMS: MS (m/z): 372.30 (M+H); ret. time: 6.31 min.

Provenance & Evidence