HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol hydrochloride → HCID 136351074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Reactant | HCID 58506482 | HCID 58506482 | — |
| Product | HCID 136351074 | HCID 136351074 | — |
Reaction Steps
A solution of 2-hydroxy-3-(2-(2-methoxyethoxy)ethoxy)benzonitrile (6 g) in EtOH/HCl (g) (150 mL) was heated to 40° C. overnight in a sealed tube. The solvent was evaporated under vacuum and the residue (7 g, crude) was used for the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045440B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-f4064b5af8634a8d83c77c9e1cbd28a0 |
| Source note | uspto-grants-2015_06 |