HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3,6-dioxaheptane → HCID 11712630, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3,6-dioxaheptane | HCID 123532 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11712630 | HCID 11712630 | 78.8% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0665 g, 0.227 mmol) and 1-bromo-2-{[2-(methyloxy)ethyl]oxy}ethane (0.055 mL, 0.405 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0843 g, 78.8%). EI-MS m/z 396 (M+) Rt (1.64 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045469B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-e1ba72d53df84c289c64e2130ee9e31e |
| Source note | uspto-grants-2015_06 |