HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Bromopropoxy)-3-fluorobenzene → HCID 11533796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Bromopropoxy)-3-fluorobenzene | HCID 23294433 | — |
| Reactant | 1-Azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol | HCID 23992385 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11533796 | HCID 11533796 | 53.1% |
Reaction Steps
Following the general procedure outlined in Example 3, 1-azabicyclo[2.2.2]oct-4-yl(diphenyl)methanol (0.0137 g, 0.0467 mmol) and 3-bromopropyl 3-fluorophenyl ether (0.0137 g, 0.0588 mmol) in 2 CH3CN/3 CHCl3 (4.0 mL) were reacted to give the desired product (0.0130 g, 53.1%). EI-MS m/z 446 (M+) Rt (2.03 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045469B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-62be8610a35a4295bc3437ad0eb74d7d |
| Source note | uspto-grants-2015_06 |