Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | Ammonium Carbonate | HCID 517111 | — |
| Reactant | 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-one | HCID 10976193 | — |
| Reactant | Water ethanol | HCID 19096565 | — |
| Product | HCID 67492974 | HCID 67492974 | — |
Reaction Steps
A mixture of 1.0 g 1-Methoxy-2,2,6,6-tetramethyl-piperidin-4-one, 527 mg potassium cyanide and 3.11 g ammonium carbonate in 21 ml water/ethanol (2:1) is stirred at 50° C. After several hours of stirring a white precipitate forms. Stirring is continued for 24 h, whereupon the precipitate is isolated by filtration. The filter cake is washed with water and ethanol and dried in vacuo. The product is obtained as a white solid, 0.99 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09045480B2 |
|---|
| Source dataset | uspto-grants-2015_06 |
|---|
| ORD ID | ord-c4c0d4d433164b1ca275e941cb1f1fa0 |
|---|
| Source note | uspto-grants-2015_06 |
|---|
