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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2167787Generated: October 30, 2026

Sulfamide → HCID 89618812, compound

https://huagongshe.com/reaction/2167787

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSulfamideHCID 82267—
ReactantHCID 89618823HCID 89618823—
ProductHCID 89618812HCID 89618812—

Reaction Steps

The title compound was prepared by the method substantially similar to that mentioned in Example-98, using 5-((R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl)-N—((S)-pyrrolidin-3-yl)pyrazolo[1,5-a]pyridine-3-carboxamide (Example-82) and Sulfamide to afford the crude, which was purified by Preparative HPLC [Column: 21.2×250×7 um, Zorbax, XDB,C-18(#22), Mobile phase-A: 10 mmol.NH4OAc in water, B:ACN, Gradient (Time/% B): 0/30, 2/30, 8/90 and Flow rate:20 mL/min] to afford 26 mg of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09045479B2
Source datasetuspto-grants-2015_06
ORD IDord-5b7e4bd2e3b4409ebb0fe7624c904cb0
Source noteuspto-grants-2015_06