HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzylamine → 4-methoxycyclohexanemethan amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzylamine | HCID 75452 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-methoxycyclohexanemethan amine | HCID 55281686 | — |
Reaction Steps
(4-Methoxyphenyl)methanamine (1 g) in ethanol (10 ml) was treated with 5% dry Rh—Al2O3 (0.5 g) under H2 (500 psi) at 60° C. for 6 hours and then at 125° C. for 26 hours. The insoluble material was filtered off and the filtrate was concentrated to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045420B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-335fdd29bf63479aa06cc46cd39c7367 |
| Source note | uspto-grants-2015_06 |