HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2168922Generated: October 30, 2026
1-Ethyl-3-(3'-dimethylaminopropyl)carbodiimide → tert-butyl (3S,5R)-3-[{[1-(4-methoxybutyl)-1H-benzimidazol-2-yl]carbonyl}(2-methylpropyl)amino)-5-(pyrrolidin-1-ylcarbonyl)piperidine-1-carboxylate
https://huagongshe.com/reaction/2168922
Participants
| Role | Name | HCID | Charge |
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| Reactant | 1-Ethyl-3-(3'-dimethylaminopropyl)carbodiimide | HCID 15908 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 1-Hydroxybenzotriazole | HCID 75771 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | (3R,5S)-(tert-butoxycarbonyl)-5-[{[1-(4-methoxybutyl)-1H-benzimidazol-2-yl]carbonyl}(2-methylpropyl)amino]piperidine-3-carboxylic acid | HCID 58355779 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | tert-butyl (3S,5R)-3-[{[1-(4-methoxybutyl)-1H-benzimidazol-2-yl]carbonyl}(2-methylpropyl)amino)-5-(pyrrolidin-1-ylcarbonyl)piperidine-1-carboxylate | HCID 58355415 | 95.4% |
Reaction Steps
(3R,5S)-1-(tert-Butoxycarbonyl)-5-[{[1-(4-methoxybutyl)-1H-benzimidazol-2-yl]carbonyl}(2-methylpropyl)amino]piperidine-3-carboxylic acid (400 mg) and pyrrolidine (59 mg) were dissolved in DMF (10 ml), WSC.HCL (217 mg) and HOBt (150 mg) were added, and the mixture was stirred at 50° C. for 12 hr. The reaction mixture was poured into 10% aqueous sodium bicarbonate, and the mixture was extracted with ethyl acetate. The extracts were combined and washed with brine and dried over anhydrous sodium sulfate. The solvent was evaporated under reduced pressure. The residue was subjected to silica gel column chromatography, and a fraction eluted with ethyl acetate-hexane (1:1-1:0) was concentrated under reduced pressure to give the object product (420 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09045436B2 |
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| Source dataset | uspto-grants-2015_06 |
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| ORD ID | ord-099c988d20014e39896e4823a18cd335 |
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| Source note | uspto-grants-2015_06 |
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