1-(4-Chlorophenyl)cyclopentanecarbonitrile → 1-(4-Chlorophenyl)-cyclopentanecarbaldehyde

HRID 2169150Notes

Reaction equation

HRID 2169150 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2([C:13]#N)[CH2:12][CH2:11][CH2:10][CH2:9]2)=[CH:4][CH:3]=1.C1(C2(C=[O:27])CCCC2)C=CC=CC=1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2([CH:13]=[O:27])[CH2:12][CH2:11][CH2:10][CH2:9]2)=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 973841-(4-Chlorophenyl)cyclopentanecarbonitrileHCID 110951241-Phenylcyclopentane-1-carbaldehyde

Product 1

HCID 214680001-(4-Chlorophenyl)-cyclopentanecarbaldehydeYield 98.23%

Procedure

1-(4-chlorophenyl)-cyclopentanecarbaldehyde (22-02) (66 g, 98.23%) was synthesized from (4-chlorophenyl)-acetonitrile (21-02) (66 g, 321.95 mmol) as a white solid as a crude product following the procedure as described for 1-phenyl-cyclopentanecarbaldehyde (22-01).

Sources & evidence

ORD record
ord-30276e9de2ea4f52a9dd419dbfbcf9de
Source dataset
uspto-grants-2015_06
Patent number
US09045486B2

Reaction notes

Loading…