HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(p-Chlorophenyl)cyclopentanemethanol → Methanesulfonic acid 1-(4-chlorophenyl)-cyclopentylmethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(p-Chlorophenyl)cyclopentanemethanol | HCID 2724017 | — |
| Reactant | (1-Phenylcyclopentyl)methyl methanesulfonate | HCID 19437914 | — |
| Product | Methanesulfonic acid 1-(4-chlorophenyl)-cyclopentylmethyl ester | HCID 86725805 | 93.08% |
Reaction Steps
Methanesulfonic acid 1-(4-chlorophenyl)-cyclopentylmethyl ester (24-02) (32 g, 93.08%) was synthesized from [1-(4-chlorophenyl)-cyclopentyl]-methanol (23-02) (25 g, 119.04 mmol) as a crude product as a yellow liquid following the procedure as described for methanesulfonic acid 1-phenyl-cyclopentylmethyl ester (24-01).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045486B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-16ed389b6b5945cd914b15602d2a9074 |
| Source note | uspto-grants-2015_06 |