HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic acid 1-(2,5-dichlorophenyl)-cyclopentylmethyl ester → Methanesulfonic acid 1-naphthalen-2-yl-cyclopentylmethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic acid 1-(2,5-dichlorophenyl)-cyclopentylmethyl ester | HCID 86725896 | — |
| Reactant | (1-Naphthalen-2-yl-cyclopentyl)-methanol | HCID 86725908 | — |
| Product | Methanesulfonic acid 1-naphthalen-2-yl-cyclopentylmethyl ester | HCID 86725909 | 54% |
Reaction Steps
Methanesulfonic acid 1-naphthalen-2-yl-cyclopentylmethyl ester (214) (16.0 g, 54.0%) was synthesized as a white solid from (1-naphthalen-2-yl-cyclopentyl)-methanol (213) (22.0 g, 97.34 mmol) following the procedure described for methanesulfonic acid 1-(2,5-dichlorophenyl)-cyclopentylmethyl ester (201).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045486B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-55f87dfe5db8478abbf21253edd321c0 |
| Source note | uspto-grants-2015_06 |