HuagongsheHuagongshe Chemistry Print Report · For research reference only
[1-(2,5-Dichlorophenyl)-cyclopentyl]-acetonitrile → (1-Naphthalen-2-yl-cyclopentyl)-acetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [1-(2,5-Dichlorophenyl)-cyclopentyl]-acetonitrile | HCID 86725897 | — |
| Reactant | Methanesulfonic acid 1-naphthalen-2-yl-cyclopentylmethyl ester | HCID 86725909 | — |
| Product | (1-Naphthalen-2-yl-cyclopentyl)-acetonitrile | HCID 86725910 | 72.67% |
Reaction Steps
(1-Naphthalen-2-yl-cyclopentyl)-acetonitrile (215) (9.0 g, 72.67%) was synthesized as a brown solid from methanesulfonic acid 1-naphthalen-2-yl-cyclopentylmethyl ester 214) (16.0 g, 52.63 mmol) following the procedure described for [1-(2,5-dichlorophenyl)-cyclopentyl]-acetonitrile (202).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09045486B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-eb1b27f9b85a40eeb64b9d1671e0c03d |
| Source note | uspto-grants-2015_06 |