2-Cyclohexen-1-OL → HCID 66747185, compound

HRID 2169997Notes

Reaction equation

HRID 2169997 reaction equation
[CH:1]1([OH:7])[CH2:6][CH2:5][CH2:4][CH:3]=[CH:2]1.[N+:8]([C:11]1[CH:18]=[CH:17][CH:16]=[C:15]([N+]([O-])=O)[C:12]=1[C:13]#[N:14])([O-:10])=[O:9]>>[CH:1]1([O:7][C:15]2[CH:16]=[CH:17][CH:18]=[C:11]([N+:8]([O-:10])=[O:9])[C:12]=2[C:13]#[N:14])[CH2:6][CH2:5][CH2:4][CH:3]=[CH:2]1

Participants

3

Reactant 2

HCID 131982-Cyclohexen-1-OLHCID 520718Dinitrobenzonitrile

Product 1

HCID 66747185HCID 66747185, compound

Procedure

Prepared as in Example 126c from cyclohex-2-enol and 2,6-dinitrobenzonitrile as a brown solid (90%). MS 245 (MH+).

Sources & evidence

ORD record
ord-be39cd419a33464bb9a444ad0637c8dd
Source dataset
uspto-grants-2015_06
Patent number
US09049878B2

Reaction notes

Loading…