p-Bromobenzenesulfonyl chloride → HCID 178501244, compound

HRID 2170026Notes

Reaction equation

HRID 2170026 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8](Cl)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[NH2:12][C@@H:13]1[CH2:18][CH2:17][C@H:16]([C:19]([O:21][CH3:22])=[O:20])[CH2:15][CH2:14]1>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH:12][C@@H:13]2[CH2:14][CH2:15][C@H:16]([C:19]([O:21][CH3:22])=[O:20])[CH2:17][CH2:18]2)(=[O:10])=[O:9])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 7396p-Bromobenzenesulfonyl chlorideHCID 178501206HCID 178501206, compound

Product 1

HCID 178501244HCID 178501244, compound

Procedure

Using a method analogous to Method A with 4-bromophenylsulfonyl chloride and methyl cis-4-aminocyclohexanecarboxylate, the title compound was obtained as a pale brown solid.

Sources & evidence

ORD record
ord-0931bcd0f6a5428aa2b1af381b2f59c2
Source dataset
uspto-grants-2015_06
Patent number
US09050329B1

Reaction notes

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