Sodium methanethiolate → HCID 89656428, compound

Participants

Reaction Steps

A mixture of Example 68c (1.51 g, 4.00 mmol) and sodium thiomethoxide (0.280 g, 4.00 mmol) in dimethylformamide (8 mL) was stirred at ambient temperature for 6 hours. The reaction mixture was partitioned with ethyl acetate and water. The organic layer was washed with saturated aqueous sodium chloride twice, dried over anhydrous sodium sulfate, filtered, and concentrated to provide the title compound (1.38 g, 100%).

Provenance & Evidence