HRID2170311
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The title compound was prepared according to the method presented for the synthesis of compound IH of Example 1 utilizing 1G and 4-chlorophenyl boronic acid. 1H NMR (400 MHz, CDCl3) δ 8.17 (s, 1H), 7.63 (d, J=8.1 Hz, 1H), 7.52 (d, J=9.0 Hz, 1H), 7.45 (d, J=8.5 Hz, 2H), 7.31-7.23 (m, 6H), 7.19 (s, 1H), 6.89 (t, J=10.0 Hz, 2H), 6.65 (d, J=8.9 Hz, 1H), 6.52 (t, J=8.9 Hz, 1H), 6.26 (d, J=5.9 Hz, 2H), 5.27 (dd, J=16.5, 8.2 Hz, 1H), 3.61 (s, 2H), 3.00 (dd, J=13.6, 9.3 Hz, 1H), 2.85 (dd, J=13.7, 7.5 Hz, 1H). MS (m/z) 535.4 [M+H]+.