HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-(methylthio)pyrimidine-4-carboxylic Acid → 5-bromo-N-methoxy-N-methyl-2-(methylthio)pyrimidine-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-(methylthio)pyrimidine-4-carboxylic Acid | HCID 291786 | — |
| Reactant | 6-acetamido-3-bromo-N-methoxy-N-methylpicolinamide | HCID 90280477 | — |
| Product | 5-bromo-N-methoxy-N-methyl-2-(methylthio)pyrimidine-4-carboxamide | HCID 90280334 | — |
Reaction Steps
The title compound (11A) was prepared according to the method presented for the synthesis of compound 1B of Example 1 utilizing 5-bromo-2-(methylthio)pyrimidine-4-carboxylic acid. MS (m/z) 292.16 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09050344B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-b8e3b75abadc47a0a4357165628072a6 |
| Source note | uspto-grants-2015_06 |