HRID2170369
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 0 °C
PROCEDURE
实验过程
Compound 30E (260 mg, 0.047 mmol) was dissolved in 10 mL of methanol and cooled to 0° C. To it was added 4N HCl/1,4-dioxane (2 ml). The reaction mixture was stirred at room temperature for overnight and concentrated to afford the title product. MS (m/z) 458.00 [M+H]+
WORKUP
后处理
- concentrationconcentrated