HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89580709, compound → HCID 72291823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89580709 | HCID 89580709 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 72291823 | HCID 72291823 | 100% |
Reaction Steps
To a solution methyl 4-(3-methylbut-2-en-2-yl)benzoate (0.2 g, 1.0 mmol) in methanol (30 mL) was added Pd/C (0.50 g). The reaction mixture was stirred at room temperature for 3 hour at 4 atm of hydrogen, after the reaction, it was filtered, and the filtrate was removed in vacuo to give pure product methyl 4-(3-methylbutan-2-yl)benzoate (0.20 g, 100%) as the colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051269B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-ab145d32eef54353af0be92cf98df3df |
| Source note | uspto-grants-2015_06 |