Formaldehyde → HCID 178482281, compound

HRID 2170563Notes

Reaction equation

HRID 2170563 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]([C:11]2[C:15]([NH:16][CH:17]3[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]3)=[CH:14][NH:13][N:12]=2)=[O:10])=[CH:4][CH:3]=1.[C:23]1(=O)CCCCC1.C=O>>[F:1][C:2]1[CH:3]=[CH:4][C:5]([NH:8][C:9]([C:11]2[C:15]([N:16]([CH:17]3[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]3)[CH3:23])=[CH:14][NH:13][N:12]=2)=[O:10])=[CH:6][CH:7]=1

Participants

4

Reactant 3

HCID 712FormaldehydeHCID 7967CyclohexanoneHCID 178522144HCID 178522144, compound

Product 1

HCID 178482281HCID 178482281, compound

Procedure

This compound was prepared in a manner analogous to the compound of Example 19 by successive reductive alkylations using firstly cyclohexanone and then formaldehyde. (LC/MS: Rt 2.77 [MH]+ 316.71).

Sources & evidence

ORD record
ord-977583377480493a91bb431bf96e51ed
Source dataset
uspto-grants-2015_06
Patent number
US09051278B2

Reaction notes

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