Acetic Anhydride → HCID 54298701, compound

HRID 217094Notes

Reaction equation

HRID 217094 reaction equation
[CH:1](C(O)=O)([C:17]([OH:19])=[O:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15]C.CC(OC(C)=O)=[O:25]>>[O:18]1[C:17](=[O:19])[CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][C:15]1=[O:25]

Participants

3

Reactant 2

HCID 7918Acetic AnhydrideHCID 14324902HCID 14324902, compound

Product 1

HCID 54298701HCID 54298701, compound

Procedure

3 g hexadecanedicarboxlic acid and 4.5 ml acetanhydride were refluxed over night. Then the solvent was removed and the crude product recrystallized from acetonitril.

Workup

  1. customThen the solvent was removed
  2. customthe crude product recrystallized from acetonitril

Sources & evidence

ORD record
ord-05227297bb31436aa5d3758f1c60fd7f
Source dataset
uspto-grants-2012_06
Patent number
US08193246B2

Reaction notes

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