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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2171029Generated: October 31, 2026

Triethylamine → HCID 71279801, compound

https://huagongshe.com/reaction/2171029

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
Reactant2-Methoxyethyl chloroformateHCID 69400—
ReactantHCID 71279377HCID 71279377—
SolventDichloromethaneHCID 6344—
ProductHCID 71279801HCID 71279801—

Reaction Steps

To a stirring solution of 4-[2-(1-Aminomethyl-cyclopropylmethoxy)-3,4-dimethoxy-phenyl]-indan-1-one (Compound 182) (150 mg, 0.272 mmol) in dichloromethane (10 mL), were added triethylamine (0.082 g, 0.811 mmol) and 2-methoxyethyl carbonochloridate (68 mg, 0.544 mmol) and the resultant reaction mixture was subjected to the conditions used in the preparation of Compound 183 to afford the title compound as a solid

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09051290B2
Source datasetuspto-grants-2015_06
ORD IDord-e960c5f6a33d43b699af65e1287482ef
Source noteuspto-grants-2015_06