HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylaniline → N-(3-chloro-2-methylphenyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylaniline | HCID 6894 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Product | N-(3-chloro-2-methylphenyl)acetamide | HCID 81969 | 100.3% |
Reaction Steps
To a solution of 3-chloro-2-methylaniline (27 g, 0.19 mol) in 270 mL of ETOH at rt was added acetic anhydride (22 mL, 0.23 mol), and the solution was stirred at rt for 2 h. The mixture was concentrated under reduced pressure to give 35 g (100%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051326B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-7db0e4284d714a27975f24b534a94031 |
| Source note | uspto-grants-2015_06 |