Triacetoxyperiodinane → HCID 57659527, compound

Participants

Reaction Steps

To a solution of 4-[5-(4-hydroxymethylfuro[3,2-c]pyridine-2-yl)-[1,2,4]oxadiazole-3-ylmethoxy]piperidine-1-carboxylic acid tert-butyl ester (Example 24, 25 mg, 58 μmol) in CH2Cl2 was added Dess-Martin periodinane (32 mg, 75 μmol). After 3 h at 20° C., the mixture was diluted with MeOH, adsorbed onto SiO2 and purified by column chromatography to furnish the title compound: RT=3.27 min; m/z (ES+)=429.1 [M+H]+.

Provenance & Evidence