HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Diphenylmethyl)azetidin-3-yl methanesulfonate → HCID 67154511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Diphenylmethyl)azetidin-3-yl methanesulfonate | HCID 2758716 | — |
| Reactant | 2-Methyl-2-buten-1-OL | HCID 6433417 | — |
| Product | HCID 67154511 | HCID 67154511 | — |
Reaction Steps
A solution of 1-benzhydrylazetidin-3-yl methanesulfonate (447 mg, 1.41 mmol) in (E)-2-methylbut-2-en-1-ol (1.2 g, 14.1 mmol) was stirred under microwaves at 110° C. for 30 minutes. After concentration to dryness, the residue was purified by chromatography on silica gel using petroleum ether/ethyl acetate (9:1) as eluent. The title product was obtained as a colorless oil (290 mg, 67%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09051321B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-28cf6ce2bf3a42f29d89f2437b3a40f3 |
| Source note | uspto-grants-2015_06 |