Cyclooctane → HCID 89500391, compound

HRID 2172356Notes

Reaction equation

HRID 2172356 reaction equation
[CH2:1]1[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:9]1(=[C:17](CCCC)[CH:18]=[O:19])CCCC[CH2:12][CH2:11][CH2:10]1>>[C:1]1(=[CH:12][CH2:11][CH2:10][CH2:9][CH2:17][CH:18]=[O:19])[CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 9266CyclooctaneHCID 89500487HCID 89500487, compound

Product 1

HCID 89500391HCID 89500391, compound

Procedure

6-cyclooctylidenehexanal is prepared according to the protocol described in Example 7 using cyclooctane in place of 2,4,4-trimethylcyclopentanone. The crude product containing cyclooctylidenehexanal is distilled under reduced pressure: its boiling point is 94° C. at 0.2 torr.

Workup

  1. distillationis distilled under reduced pressure

Sources & evidence

ORD record
ord-87738293fbe247d598461f49048eecb3
Source dataset
uspto-grants-2015_06
Patent number
US09051531B2

Reaction notes

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