HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2172391Generated: October 31, 2026
Trifluoroacetic acid → HCID 89388365, compound
https://huagongshe.com/reaction/2172391
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 89388363 | HCID 89388363 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 89388365 | HCID 89388365 | — |
Reaction Steps
A solution of Example 215B (200 mg, 0.54 mmol) in dichloromethane (20 ml) was added TFA (5 mL). The mixture was stirred at 40° C. overnight. The reaction mixture was concentrated and the crude product was used in the next step without further purification. MS (DCI/NH3) m/z 474 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09051327B2 |
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| Source dataset | uspto-grants-2015_06 |
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| ORD ID | ord-568f834a21f741a78fc97c63f5280309 |
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| Source note | uspto-grants-2015_06 |
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