HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → N-phenyl-3-(phenylsulphanyl)prop-2-enimidoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | N-phenyl-3-(phenylthio)acrylamide | HCID 68865691 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | N-phenyl-3-(phenylsulphanyl)prop-2-enimidoyl chloride | HCID 86702346 | — |
Reaction Steps
Thus, for example, IN 2003-MU444 describes the reaction of N-cyclohexyl-5-hydroxypentanamide with phosphorus pentachloride to give 5-chloro-N-cyclohexylpentaneimidoyl chloride. WO 2007/063702 provides the reaction of N-phenyl-3-(phenylsulphanyl)acrylamide with thionyl chloride and catalytical amounts of N,N-dimethylformamide to give N-phenyl-3-(phenylsulphanyl)prop-2-enimidoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09055743B2 |
| Source dataset | uspto-grants-2015_06 |
| ORD ID | ord-6f41368e816f4109beacab54f612f492 |
| Source note | uspto-grants-2015_06 |